9-fluorenemethanol CAS NO 24324-17-2

9-fluorenemethanol (CAS NO 24324-17-2)

Specifications:

Preparation:

A method for preparing 9-fluorene methanol, which comprises the following steps: 

Step 1. Synthesize 9-fluorene methanol, which comprises the following two steps:   

    step 1.1. Under the action of a catalyst and a co-catalyst, make fluorene 9 One hydrogen on the upper part is removed in the form of a proton, and the generated fluorene anion reacts with ethyl formate to generate 9-fluorene formaldehyde; 

    step 1.2. Using a reducing agent, 9-fluorene formaldehyde is reduced by a reduction reaction to form a crude product of 9-fluorene methanol 

Step 2. Use the solvent two-step purification method to purify 9-fluorene methanol, which includes the following two steps: 

    step 2.1. The crude product of 9-fluorene methanol is heated and dissolved in the first solvent in a certain proportion, and the insoluble matter is filtered out , The filtrate is cooled, the crystals are precipitated, and then filtered and vacuum dried to obtain the primary purification product of 9-fluorene methanol after the first step purification; 

    step 2.2. The primary purification product of 9-fluorene methanol after the first step purification , Dissolved in the second solvent according to a certain proportion, filtered out the insoluble matter, and then precipitated crystals on the filtrate by the elution method. After cooling, filtered and dried in vacuum to obtain purified 9-fluorene methanol.

Hot Tags: 9-fluorenemethanol cas no 24324-17-2, China, manufacturers, suppliers, factory, White Crystal Powder 9 fluorenylmethanol, 9 Hydroxymethyl fluorene, Biopharmaceutical Raw Materials 9 fluorenemethanol, 9H fluoren 9 ylmethanol, 9 fluorenemethanol C14H12O, 9 fluorenylmethanol